2

D

Deuterium

2.1040

88

Ra

Radium

(226)

7

N

Nitrogen

14.007

90

Th

Thorium

232.04

8

O

Oxygen

15.999

7

N

Nitrogen

14.007

39

Y

Yttrium

88.906

19

F

Fluorine

18.998

57

La

Lanthanum

138.91

31

Ga

Gallium

69.723

57

La

Lanthanum

138.91

7

N

Nitrogen

14.007

52

Te

Tellurium

127.60

 

Patents


 

Patent 6,334,949 “Process for the Removal of Carbonyl Sulfide from Liquefied Petroleum Gas” T.J. Bruno, A.F. Lagalante (January 1, 2002).

 

Publications


undergraduate student co-author

graduate student co-author

 

1

 

R.E. Sievers, S.B. Turnipseed, L. Huang and A.F. Lagalante "Volatile Barium ß-Diketonates for Use as MOCVD Precursors" Coordination Chemistry Reviews  128(1-2), 285-291 (1993).

2

 

B.M. Hybertson, K.S. Rutledge, C.J. Beehler, J.E. Repine, A.F. Lagalante and R.E. Sievers "Pulmonary Drug Delivery of Fine Aerosol Particles from Supercritical Fluids" Journal of Aerosol Medicine  6(4), 275-283 (1993).

3

 

B.N. Hansen, A.F. Lagalante, T.J. Bruno and R.E. Sievers "High-Pressure Cell for Solubility Measurements in Supercritical Fluids" Reviews of Scientific Instrumentation 65(6), 2112-2114 (1994).

4

 

A.F. Lagalante, B.N. Hansen,  T.J. Bruno and R.E. Sievers "Solubility of Copper(II) and Chromium(III) ß-Diketonates in Supercritical Carbon Dioxide" Inorganic Chemistry  34(23), 5781-5785 (1995).

5

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A.F. Lagalante, R.J. Jacobson and T.J. Bruno "UV/Vis Spectroscopic Evaluation of 4-Nitropyridine N-Oxide as a Solvatochromic Indicator for the Hydrogen-Bond Donor Ability of Solvents" Journal of Organic Chemistry  61(18), 6404-6406 (1996).

6

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A.F. Lagalante and T.J. Bruno “Modeling the Water-Supercritical CO2 Partition Coefficients of Organic Solutes using a Linear Solvation Energy Relationship” Journal of Physical Chemistry, B 102(6), 907-909 (1998).

7

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A.F. Lagalante, R.L. Hall and T.J. Bruno “Kamlet-Taft Solvatochromic Parameters of the Sub- and Supercritical Fluorinated Ethane Solvents” Journal of Physical Chemistry, B 102(34), 6601-6604 (1998).

8

 

B.F. Graham, J.M. Harrowfield, R.D. Trengrove, A.F. Lagalante and T.J. Bruno “Solubility of p-t-Butylcalix[n]arenes (n=4,6,8) in Supercritical Carbon Dioxide: A Comparison of Static and Dynamic Measurement Techniques” Fluid Phase Equilibria  151(2), 829-838 (1998).

9

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A.F. Lagalante, A.M. Clarke and T.J. Bruno “Modeling the Water-R134a Partition Coefficients of Organic Solutes using a Linear Solvation Energy Relationship” Journal of Physical Chemistry, B 102(44), 8889-8892 (1998). 

10

 

A.F. Lagalante, C. Wood, A.M. Clarke and T.J. Bruno “The Kamlet-Taft Solvatochromic Parameters for 25 Glycol Ether Solvents and Glycol Ether Aqueous Solutions” Journal of Solution Chemistry 27(10), 887-900 (1998).

11

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A.F. Lagalante, A.M. Clarke and T.J. Bruno “Modeling the Water-R143a Partition Coefficients of Organic Solutes using a Linear Solvation Energy Relationship” Journal of Physical Chemistry, B 103(34), 7319-7323 (1999).

12

 

A.F. Lagalante “Atomic Absorption Spectroscopy: A Tutorial Review” Applied Spectroscopy Reviews 34(3), 173-190 (1999).

13

 

A.F. Lagalante “Atomic Emission Spectroscopy: A Tutorial Review” Applied Spectroscopy Reviews 34(3), 191-207 (1999).

14

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A.F. Lagalante, M. Spadi and T.J. Bruno “Kamlet-Taft Solvatochromic Parameters of Eight Alkanolamines” Journal of Chemical and Engineering Data  45(2), 382-385 (2000).

15

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W.C. Andersen, R.E. Sievers, A.F. Lagalante, and T.J. Bruno “Solubilities of Cerium(IV), Terbium(III), and Iron(III) ß-Diketonates  in Supercritical Carbon Dioxide” Journal of Chemical and Engineering Data  46(5), 1045-1049 (2001). 

16

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B.F. Graham, J.M. Harrowfield, R.D. Trengrove, A.F. Lagalante and T.J. Bruno “Host:Guest Complex Formation Between Carbon Dioxide and the p-t-Butylcalixarenes” Journal of Inclusion Phenomena 43(3-4), 179-182 (2002).

17

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A.F. Lagalante, A. Abdulagatov, and T.J. Bruno “Kamlet-Taft Thermosolvatochromic Parameters of Hydrofluoroethers and Hydrofluoroether Azeotropic Mixtures” Journal of Chemical and Engineering Data  47(1), 47-51 (2002).

18

 

A.F. Lagalante and M.E. Montgomery “Analysis of Terpenoids from Tsuga Species by Solid-Phase Microextraction/Gas Chromatography/Ion-Trap Mass Spectrometry” Journal of Agricultural and Food Chemistry 51(8), 2115-2120 (2003).

19

 

A.F. Lagalante and M.A. Felter “Silylation of acrylamide for analysis by solid-phase microextraction/gas chromatography/ion-trap mass spectrometry”  Journal of Agricultural and Food Chemistry 52(12), 3744-3748 (2004).

20

 

A.F. Lagalante, N. Lewis, M.E. Montgomery and K.S. Shields “Temporal and Spatial Variation of Terpenoids in Eastern Hemlock (Tsuga canadensis) in Relation to Feeding by Adelges tsugaeJournal of Chemical Ecology 32(11), 2389-2403 (2006).

21

 

T. Rowhani and A.F. Lagalante “A Colorimetric Assay for the Determination of Polyhexamethlene Biguanide in Pool and Spa Water using Nickel-Nioxime” Talanta 71(2), 964-970 (2007).

22

 

A.F. Lagalante and P.W. Greenbacker "Flow injection analysis of imidacloprid in natural waters and agricultural matrixes by photochemical dissociation, chemical reduction, and nitric oxide chemiluminescence detection" Analytica Chimica Acta 590, 151-158 (2007).

23

 

J. Tierney, N. Colasante, J. Eagles, S. Kelly, G. Lehmike, O. Lucas, C. Mannikarottu, O. Mehmood, M.D. Nguyen, V. Raj, J. Tsai, V. Koyfman, L.M. Mascavage, and A.F. Lagalante "A Comparison of Substituent Effects Using 13C Chemical Shifts for a Series of Substituted 2-Phenyl-3-pyridyl-1,3-thiazolidin-4-ones Compared to Similarly Substituted 1,3-thiazolidin-4-ones" Heterocyclic Communications 13(6), 335-342 (2007).

24

 

A.F. Lagalante, M.E. Montgomery, F. Calvosa and M. Mirzabeigi “Characterization of Terpenoid Volatiles from Cultivars of Eastern Hemlock (Tsuga canadensis)” Journal of Agricultural and Food Chemistry 55(26), 10850-10856 (2007).

25

 

A.F. Lagalante and T.D. Oswald “Analysis of Polybrominated Diphenyl Ethers (PBDEs) by Liquid Chromatography with Negative-Ion Atmospheric Pressure Photoionization Tandem Mass Spectrometry (LC/NI-APPI/MS/MS): Application to House Dust” Analytical and Bioanalytical Chemistry 391(6), 2249-2256 (2008).

26

 

J. Tierney, V. Koyfman, K. Cannon, L.M. Mascavage, and A.F. Lagalante "A Second Study - Predicting the 13C Chemical Shifts For a Series of Substituted-3-(4-methoxyphenyl)-2-phenyl-1,3-thiazolidin-4-ones" Heterocyclic Communications 14(6), 452-460 (2008).

27

 

A.F. Lagalante T.D. Oswald, and F.C. Calvosa “Polybrominated Diphenyl Ether (PBDE) Levels in Dust from Previously Owned Automobiles at United States Dealerships” Environment International 35, 539-544 (2009).

28

 

A.M. Grannas and A.F. Lagalante “So These Numbers Really Mean Something? A Role Playing Scenario-Based Approach to the Undergraduate Instrumental Analysis Laboratory” Journal of Chemical Education 87(4), 416-418 (2010).

 

Presentations


 

 

A.F. Lagalante "Analysis of Polybrominated Diphenyl Ethers (PBDEs) in Indoor Environments" presented at the Shimadzu Workshop on Emerging Applications in Mass Spectrometry, Villanova, PA, March 4, 2009.

R.S. Cowles and A.F. Lagalante “Activity And Persistence of Systemic Insecticides for Managing Hemlock Woolly Adelgids” presented at the 20th USDA Interagency Research Forum on Gypsy Moth and Other Invasive Species, Annapolis, MD, January 16-19, 2009.

A.F. Lagalante, T.D. Oswald, F.C. Calvosa "Analysis of Polybrominated Diphenyl Ethers (PBDEs) by Liquid Chromatography with Negative-Ion Atmospheric Pressure Photoionization Tandem Mass Spectrometry (LC/NI-APPI/MS/MS).  Method Validation and Application to Automobile Dust" presented at the SETAC North America 29th Annual Meeting, Tampa, FL,  November 16-20, 2008.

A.F. Lagalante (Invited talk) “New Techniques to Evaluate Imidacloprid Metabolites” presented at the 4th Hemlock Woolly Adelgid Symposium, Hartford, CT, February 12-14, 2008.

A.F. Lagalante (Invited talk) “Evaluating Hemlock Terpenoids” presented at the 4th Hemlock Woolly Adelgid Symposium, Hartford, CT, February 12-14, 2008.

F.C. Calvosa and A.F. Lagalante “Determination of polybrominated diphenyl ethers (PBDEs) in dust by SFE-GC-EI/MS/MS and GC-NCI/MS” presented at 28th Annual Meeting of SETAC North America, Milwaukee, WI, November 11-14, 2007.

 

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K.L. Hess, M. Papalaskari, R. Weinstein, R. Styer, T. Way and A.F. Lagalante "Creation of the Milwaukee School of Magic" Frontiers in Education Conference, Session S1F, Milwaukee, WI, October 10-13, 2007.

 

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M. Papalaskari, K.L. Hess, A.F. Lagalante, N. Nadi, R. Styer, T. Way and R. Weinstein "Work in Progress - Engineering the Magic School Creativity and Innovation in Context" Frontiers in Education Conference, Session S2B, Milwaukee, WI, October 10-13, 2007.

   

A.F. Lagalante (Invited talk) “Cross-Curriculum implementation of art in chemistry at Villanova University” presented at Division of Chemical Education for the 234th American Chemical Society National Meeting, Boston, MA, August 19-23, 2007.

T. Oswald and A.F. Lagalante “Novel approaches to sampling and detection of PBDEs in dust using SPME and APPI-LC-MS-MS” presented at Division of Analytical Chemistry for the 234th American Chemical Society National Meeting,  Boston, MA, August 19-23, 2007.

A. Norbutus and A.F. Lagalante “Spectroscopic examination of a Dutch genre oil painting” presented at Division of Analytical Chemistry for the 234th American Chemical Society National Meeting, Boston, MA, August 19-23, 2007.

F.C. Calvosa and A.F. Lagalante “Determination of polybrominated diphenyl ethers (PBDEs) in dust by SFE-GC-MS-MS” presented at Division of Analytical Chemistry for the 234th American Chemical Society National Meeting, Boston, MA, August 19-23, 2007.

F. Cook and A.F. Lagalante “LC-MS-MS analysis of imidacloprid and metabolites in hemlock trees” presented at Division of Agrochemicals for the 234th American Chemical Society National Meeting, Boston, MA, August 19-23, 2007.

J. Tierney and A.F. Lagalante “The mass spectra and fragmentation patterns for some 4-thiazolidinones” presented at the American Chemical Society Middle Atlantic Regional Meeting, Ursinus College, Collegeville, PA, May 16 - 18, 2007.

A. Grannas and A.F. Lagalante “So these numbers really mean something?: A role-playing, collaborative approach to the instrumental analysis laboratory” presented in the  Recent Advances in Teaching Analytical Chemistry Session at the 231st American Chemical Society National Meeting, Atlanta, GA, March 26-30, 2006

F.C. Calvosa, M.N. Mirzabeigi, A.F. Lagalante, M.E. Montgomery and K.S. Shields, “Multivariate Statistical Analysis of Hemlock (Tsuga) Volatiles by SPME/GC/MS: Insights into the Phytochemistry of the Hemlock Woolly Adelgid (Adelges tsugae Annand)” presented at The Eighth International Symposium on Advances in Extraction Techniques (ExTech), York, GB, February 5-8, 2006. 

P. Greenbacker, J. Jones, A.F. Lagalante, R. Turcotte and B. Onken, “Measurement of Imidacloprid in Xylem Fluid from Eastern Hemlock (Tsuga canadensis) by Derivatization/GC/MS and ELISA”, presented at The Eighth International Symposium on Advances in Extraction Techniques (ExTech), York, GB, February 5-8, 2006.

F.C. Calvosa, M.N. Mirzabeigi, A.F. Lagalante, M.E. Montgomery and K.S. Shields, “Multivariate Statistical Analysis of Hemlock (Tsuga) Volatiles by SPME/GC/MS: Insights into the Phytochemistry of the Hemlock Woolly Adelgid (Adelges tsugae Annand)” presented at the 17th USDA Interagency Research Forum on Gypsy Moth and Other Invasive Species, Annapolis, MD, January 10-14, 2006.

P. Greenbacker, J. Jones, A.F. Lagalante, R. Turcotte and B. Onken, “Measurement of Imidacloprid in Xylem Fluid from Eastern Hemlock (Tsuga canadensis) by Derivatization/GC/MS and ELISA”, presented at the 17th USDA Interagency Research Forum on Gypsy Moth and Other Invasive Species, Annapolis, MD, January 10-14, 2006.

Michael E. Montgomery, Anthony F. Lagalante, and Kathleen S. Shields, “Resistance of Hemlock to Adelges tsugae: Promising New Developments” presented at the Third Symposium on Hemlock Woolly Adelgid in the Eastern United States, Renaissance Asheville Hotel, February 1-3, 2005. 

A.F. Lagalante, N.M. Lewis, M.E. Montgomery and K.S. Shields, “Role of Terpenoids in Hemlock Resistance to HWA” presented at the 15th USDA Interagency Research Forum on Gypsy Moth and Other Invasive Species, Annapolis, MD, January 13-16, 2004.

A.F. Lagalante, and M.A. Felter, “Analysis of Acrylamide by SPME/GC/MS” presented at the 36th American Chemical Society Middle Atlantic Regional Meeting (MARM), Princeton University, Princeton, NJ, June 8-11, 2003.

B. Ryals, D. Hokien-Carey, A.F. Lagalante, and B. Whitmann, “Phytoremediation of Methyl Tertiary-Butyl Ether (MTBE) in River Birch Saplings” presented at the 36th American Chemical Society Middle Atlantic Regional Meeting (MARM), Princeton University, Princeton, NJ, June 8-11, 2003.

A.F. Lagalante and M.E. Montgomery “Analysis of Hemlock (Tsuga) Volatiles by SPME/GC/MS” The Pittsburgh Conference, Orlando, FL, March 9-14, 2003.

M.E. Montgomery, A.F. Lagalante, C. Sclar, and B.K. Maynard, “Comparative Resistance of Hemlock Species to Adelges tsugae (Homoptera: Adelgidae)” National Entomological Society Meeting, Fort Lauderdale, FL, November 17-22, 2002.

W.C. Andersen, R.E. Sievers, A.F Lagalante and T.J. Bruno “Solubilities and Extraction of Iron(III), Cerium(IV) And Terbium(III) β-Diketonates In Supercritical Carbon Dioxide” 44th Rocky Mountain Conference on Analytical Chemistry, Denver, CO, July 28-August 1, 2002.

A.F. Lagalante and T.J Bruno “Solvatochromic Parameters of Alternative Refrigerants” Symposium in Honor of Professor Daniel E. Martire, Georgetown University, Washington, DC, May 4-5, 2001.

A.F Lagalante, A. Abdulagatov and T.J. Bruno “Thermosolvatochromic Parameters of Fluorinated Ethers” 14th Symposium on Thermophysical Properties, Boulder, CO, June 25-30, 2000.

M. Spadi, A.F Lagalante and T.J. Bruno “Solution Thermodynamics of Propylene Glycol Phenyl Ether Determined by Gas-Liquid Chromatography” 14th Symposium on Thermophysical Properties, Boulder, CO, June 25-30, 2000.

A.F Lagalante and T.J. Bruno “Kamlet-Taft Parameters and Predictive Models for the Design and Selection of Alternative Supercritical Solvents” 14th Symposium on Thermophysical Properties, Boulder, CO, June 25-30, 2000.

W.C. Andersen, R.E. Sievers, A.F Lagalante and T.J. Bruno “Solubilities and Modeling of Iron(III), Cerium(IV) And Terbium(III) β-Diketonates In Supercritical Carbon Dioxide” 14th Symposium on Thermophysical Properties, Boulder, CO, June 25-30, 2000.

B.F. Graham, J.M. Harrowfield, R.D. Trengove, A.F. Lagalante, T.J. Bruno “Solubility of p-t-butylcalix[n]arenes in Supercritical Carbon Dioxide and their Correlation with Pseudo Solubilities from Supercritical Fluid Extraction” 13th Symposium on Thermophysical Properties, Boulder, CO, June 1997.

A.F Lagalante and T.J. Bruno “The Kamlet-Taft Parameters of the Fluorinated Ethane Solvents and their use in Linear Solvation Energy Relationships to Model Water-Supercritical Fluid Partitioning” 8th International Symposium of Supercritical Fluid Chromatography and Extraction, St. Louis, MO, July 12-16, 1998.

A.F Lagalante and T.J. Bruno “A Chemical Approach to Phase Equilibrium: Determination of the Kamlet-Taft Parameters for Alternative Supercritical Fluid Solvents” AIChE National Meeting, Chicago, IL, November 1996.

A.F Lagalante, B.M. Hyberson and R.E. Sievers “Pulmonary Supercritical Fluid Drug Delivery of Vitamin E” 37th Rocky Mountain Conference on Analytical Chemistry, Denver, CO, July 1995.